Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → HCID 69136183, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| 반응물 | tert-Butyl (1S,2R)-1-benzyl-2-hydroxy-3-[(3-methoxybenzyl)amino]propylcarbamate | HCID 57512771 | — |
| 생성물 | HCID 69136183 | HCID 69136183 | — |
반응 단계
1-tert-butyl (1S,2R)-1-benzyl-2-hydroxy-3-[(3-methoxybenzyl)amino]propylcarbamate (XXXIV, EXAMPLE 5, 5.4 g) and dioxane-hydrochloric acid (20 ml, 4 N) are mixed. The reaction mixture is stirred at 20–25° for 30 minutes then poured into stirred ether (300 ml). The product is filtered and dried under reduced pressure to give the title compound, M+H=435.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07144897B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-a6c5d12b119445ada3449a279e8e5e9b |
| 출처 메모 | uspto-grants-2006_12 |