Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cesium Chloride → 2-Chloro-4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cesium Chloride | HCID 24293 | — |
| 반응물 | 4-[6-(4-Trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazol-2-ylamine | HCID 10091650 | — |
| 촉매 | Cuprous chloride | HCID 62652 | — |
| 생성물 | 2-Chloro-4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazole | HCID 10476517 | — |
반응 단계
The title compound was prepared in an analogous manner to the conditions of Example 91 by reacting 4-[6-(4-trifluoromethyl-phenyl)-pyrimidin-4-yloxy]-benzothiazol-2-ylamine (Example 65) with CsCl and CuCl. MS (ESI, pos. ion.) m/z: 408 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07144888B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-d5a40e3dd74b44f0bbeb53c35f3a7969 |
| 출처 메모 | uspto-grants-2006_12 |