Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acrylic Acid → t-Butyl acrylate acrylic acid 3-hydroxypropyl methacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acrylic Acid | HCID 6581 | — |
| 반응물 | Propylene glycol methyl ether acetate | HCID 7946 | — |
| 반응물 | tert-Butyl acrylate | HCID 15458 | — |
| 반응물 | 3-Hydroxypropyl methacrylate | HCID 17694 | — |
| 촉매 | Azobisisobutyronitrile | HCID 6547 | — |
| 생성물 | t-Butyl acrylate acrylic acid 3-hydroxypropyl methacrylate | HCID 86601184 | 118.6% |
반응 단계
10 g of t-butylacrylate, 4 g of acrylic acid, 6 g of 3-hydroxypropyl methacrylate and 0.4 g of AIBN were added to 200 g of PGMEA, and were then polymerized at 60° C. for 8 hours. After completion of the polymerization, the mixture was precipitated in ether, filtered, and dried in vacuo to yield 17 g of t-butyl acrylate-acrylic acid-3-hydroxypropyl methacrylate copolymer, as a white solid, represented by Formula 2 below:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07147994B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-eb8c73245c1e4136871d0a3dd29432be |
| 출처 메모 | uspto-grants-2006_12 |