P-Anisidine → N-4-methoxyphenyl-N'-cyano-O-phenylisourea
반응식
C1C=CC(O[C:8]([O:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[N:9][C:10]#[N:11])=CC=1.[CH3:19][O:20][C:21]1[CH:27]=[CH:26][C:24]([NH2:25])=[CH:23][CH:22]=1>C(O)(C)C>[CH3:19][O:20][C:21]1[CH:27]=[CH:26][C:24]([NH:25][C:8](=[N:9][C:10]#[N:11])[O:12][C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)=[CH:23][CH:22]=1참가 물질
4
실험 절차
A slurry of diphenyl cyancarbonimidate (1 g) in isopropanol (10 mL) was treated with 4-methoxyaniline (517 mg). After stirring at room temperature for a further 2.5 hours the reaction mixture was filtered. The insoluble material was washed with isopropanol to give the title compound (778 mg) as a white solid, which was used without further purification.
후처리
- filtrationwas filtered
- washThe insoluble material was washed with isopropanol
출처 및 근거
- ORD 기록
- ord-c5d16a2e556b4d6f8942453347cd673f
- 출처 데이터셋
- uspto-grants-2006_12
- 특허 번호
- US07148215B2
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