1-Chloro-3-iodopropane → HCID 11075029, 화합물

반응식

[N:1]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[C:4](=[O:11])[NH:3][N:2]=1.[Cl:12][CH2:13][CH2:14][CH2:15]I>>[Cl:12][CH2:13][CH2:14][CH2:15][N:3]1[C:4](=[O:11])[C:5]2[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=2[N:1]=[N:2]1

참가 물질

반응물 2

HCID 813631-Chloro-3-iodopropane

HCID 1354087931,2,3-Benzotriazin-4-one

생성물 1

HCID 11075029HCID 11075029, 화합물

실험 절차

3-(3-chloropropyl)-1,2,3-benzotriazin-4(3H)one was prepared according to the general procedure outlined in example 6, step 1. Starting from 1,2,3-benzotriazin-4(3H)one (2 g, 13.6 mmol) and 1-chloro-3-iodopropane (1.6 mL, 14.95 mmol), 1.57 g (52%); yellow solid; m.p. 69° C., MS: 223.9 (M+H)+

출처 및 근거

ORD 기록: ord-8ece5ebbde11416eb52f0e1bbf7c2b8d
출처 데이터셋: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07148235B2

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