3-Fluoro-4-methoxybenzoic acid → HCID 135443301, 화합물

HRID 858227노트

반응식

HRID 858227 반응식
[Br:1][C:2]1[C:8]([O:9]C)=[CH:7][C:5]([NH2:6])=[C:4]([O:11][CH3:12])[CH:3]=1.[F:13][C:14]1[CH:15]=[C:16]([CH:20]=[CH:21][C:22]=1[O:23]C)C(O)=O>>[Br:1][C:2]1[C:8]([OH:9])=[CH:7][C:5]2[N:6]=[C:12]([C:16]3[CH:20]=[CH:21][C:22]([OH:23])=[C:14]([F:13])[CH:15]=3)[O:11][C:4]=2[CH:3]=1

참가 물질

3

반응물 2

HCID 27334013-Fluoro-4-methoxybenzoic acidHCID 164901364-Bromo-2,5-dimethoxyaniline

생성물 1

HCID 135443301HCID 135443301, 화합물

실험 절차

The title compound was prepared in substantially the same manner as described in Example 16, from 4-bromo-2,5-dimethoxyaniline, and 3-fluoro-4-methoxybenzoic acid and was obtained as a white solid, m.p. 224–226° C.; MS m/e 322 (M−H)+.

후처리

  1. customwas obtained as a white solid, m.p. 224–226° C.

출처 및 근거

ORD 기록
ord-3833b69be985456b9ee56abc0413acac
출처 데이터셋
uspto-grants-2006_12
특허 번호
US07148247B2

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