Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2,3-Difluorophenyl)boronic acid → (2',3'-Difluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2,3-Difluorophenyl)boronic acid | HCID 2734333 | — |
| 반응물 | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| 생성물 | (2',3'-Difluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69592780 | 91.9% |
반응 단계
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) (3.64 g, 10 mmol) and 2,3-difluorobenzene boronic acid (2.35 g, 14.9 mmol) according to the general procedure B. Obtained as a yellow solid (3.22 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07151098B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-ef3894fc7dea470d926036dbd5890080 |
| 출처 메모 | uspto-grants-2006_12 |