Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromopyridine → (2-Nitro-4-pyridin-2-ylethynyl-phenyl)-carbamic acid tert.-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromopyridine | HCID 7973 | — |
| 반응물 | tert-Butyl (4-ethynyl-2-nitrophenyl)carbamate | HCID 23554338 | — |
| 생성물 | (2-Nitro-4-pyridin-2-ylethynyl-phenyl)-carbamic acid tert.-butyl ester | HCID 69592858 | 86.3% |
반응 단계
Prepared from (4-ethynyl-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example F2) (262 mg, 1.0 mmol) and 2-bromopyridine (0.15 mL, 1.6 mmol) according to the general procedure F. Obtained as a yellow solid (293 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07151098B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-dc0bc078b7fb4ef4af8928a193087666 |
| 출처 메모 | uspto-grants-2006_12 |