HCID 69592854, 화합물 → HCID 69592814, 화합물

HRID 859337노트

반응식

HRID 859337 반응식
[C:1]([O:5][C:6](=[O:28])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][C:17]([F:20])=[CH:16][C:15]=2[O:21][CH2:22][O:23][CH3:24])=[CH:10][C:9]=1[N+:25]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>[Pd]>[C:1]([O:5][C:6](=[O:28])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][C:17]([F:20])=[CH:16][C:15]=2[O:21][CH2:22][O:23][CH3:24])=[CH:10][C:9]=1[NH2:25])([CH3:4])([CH3:2])[CH3:3]

참가 물질

3

반응물 1

HCID 69592854HCID 69592854, 화합물

생성물 1

HCID 69592814HCID 69592814, 화합물

시약·촉매·용매 1

HCID 23938Palladium촉매

실험 절차

Prepared from (4′-fluoro-2′-methoxymethoxy-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example B14) by catalytic hydrogenation with Pd/C according to the general procedure G (method a). Obtained as a light purple foam (577 mg).

출처 및 근거

ORD 기록
ord-88d454519e3546ab9057fb3b7e71c4de
출처 데이터셋
uspto-grants-2006_12
특허 번호
US07151098B2

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