Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2',4'-Difluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester → Carbamic acid,(3-amino-2',4'-difluoro[1,1'-biphenyl]-4-yl)-,1,1-dimethylethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2',4'-Difluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69592801 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | Carbamic acid,(3-amino-2',4'-difluoro[1,1'-biphenyl]-4-yl)-,1,1-dimethylethyl ester | HCID 69592785 | — |
반응 단계
Prepared from (2′,4′-difluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example B15) by catalytic hydrogenation with Pd/C according to the general procedure G (method a). Obtained as a light yellow solid (1.77 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07151098B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-11e03ba7c64f477fbc423f7d4f9c9ea2 |
| 출처 메모 | uspto-grants-2006_12 |