HCID 22224885, 화합물 → HCID 69592846, 화합물

HRID 859360노트

반응식

HRID 859360 반응식
[C:1]([C:3]1[S:7][C:6]([C:8]([O:10]CC)=O)=[CH:5][CH:4]=1)#[N:2].[C:13]([O:16][C:17]([CH3:20])([CH3:19])[CH3:18])(=[O:15])[CH3:14].[Li]>>[C:17]([O:16][C:13](=[O:15])[CH2:14][C:8]([C:6]1[S:7][C:3]([C:1]#[N:2])=[CH:4][CH:5]=1)=[O:10])([CH3:20])([CH3:19])[CH3:18]

참가 물질

3

반응물 2

HCID 22224885HCID 22224885, 화합물HCID 86586795Lithium Tert-butyl Acetate

생성물 1

HCID 69592846HCID 69592846, 화합물

실험 절차

Prepared from ethyl 5-cyano-2-thiophenecarboxylate [CAS-No. 67808-35-9] by treatment with lithium tert.-butyl acetate according to general procedure H (method b). Obtained as a yellow solid (6.66 g).

출처 및 근거

ORD 기록
ord-73ac11849b2a49878de8463bbfe0143e
출처 데이터셋
uspto-grants-2006_12
특허 번호
US07151098B2

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