참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phenylacetylene | HCID 10821 | — |
| 반응물 | 4-Bromobenzaldehyde | HCID 70741 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 4-(Phenylethynyl)benzaldehyde | HCID 609908 | 63% |
반응 단계
4-Bromobenzaldehyde (370 mg, 2 mmol), phenylacetylene (306 mg, 3 mmol) and tetrakistriphenylphosphine palladium (45 mg) were dissolved in triethylamine (4 ml), and the obtained solution was stirred at 80° C. in argon atmosphere for 24 hours. The solvent was evaporated, and the product was purified by the silica gel column chromatography to obtain 4-(2-phenylethynyl)benzaldehyde (yield: 258 mg, 63%)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07153850B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_12 |
|---|
| ORD ID | ord-c6503ad896b248589942d3d07b72e6b8 |
|---|
| 출처 메모 | uspto-grants-2006_12 |
|---|
