HCID 69373820, 화합물 → HCID 69375686, 화합물
반응식
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]([C:10]2[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][CH:11]=2)[OH:9])=[N:6][CH:7]=1>CCOC(C)=O.O=[Mn]=O>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]([C:10]2[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][CH:11]=2)=[O:9])=[N:6][CH:7]=1참가 물질
4
실험 절차
To a solution of (5-bromo-pyridin-2-yl)-(4-methoxy-phenyl)-methanol (1.0 eq.) in EtOAc (0.2M) was added MnO2 (3.0 eq.). The mixture was stirred for 1 h, filtered on celite and concentrated to afford the title compound as a white solid.
후처리
- filtrationfiltered on celite
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-e140339956ab4924a9d9fa05b001ff55
- 출처 데이터셋
- uspto-grants-2006_12
- 특허 번호
- US07153968B2
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