Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibenzoylmethane → Ethyl Acetoacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibenzoylmethane | HCID 8433 | — |
| 반응물 | 2-Acetylcyclohexanone | HCID 13400 | — |
| 반응물 | Ethyl 2-oxocyclopentanecarboxylate | HCID 69136 | — |
| 반응물 | Ethyl 4-methyl-2-oxocyclohexanecarboxylate | HCID 98162 | — |
| 반응물 | 2-Acetylcyclopentanone | HCID 98471 | — |
| 생성물 | Ethyl Acetoacetate | HCID 8868 | — |
반응 단계
Using the same apparatus and procedure as described in Example 1, the onset temperature for a one gram sample of 82.5% di-2-ethylhexyl peroxydicarbonate diluted in OMS was measured. The procedure was repeated with separate samples of the above solution to which ethyl-2-cyclohexanone carboxylate, 2-acetyl cyclohexanone, 2-acetyl cyclopentanone, methyl-2-cycloheptanone carboxylate, ethyl-2-oxocyclopentane carboxylate, dibenzoyl methane, and ethyl-4-methyl-2-cyclohexanone-1-carboxylate had been added. The results are shown in Table II. Results obtained with ethyl acetoacetate, which is disclosed in the prior art, are included for comparison.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05714626 |
| 출처 데이터셋 | uspto-grants-1998_02 |
| ORD ID | ord-71507d96d87d401a998478b7395a67e2 |
| 출처 메모 | uspto-grants-1998_02 |