Trimethyl phosphite → 2-Dimethoxyphosphorylmethyl-5-nitrothiophene

HRID 861884노트

반응식

HRID 861884 반응식
Br[CH2:2][C:3]1[S:4][C:5]([N+:8]([O-:10])=[O:9])=[CH:6][CH:7]=1.[CH3:11][O:12][P:13]([O:16]C)[O:14][CH3:15]>>[CH3:11][O:12][P:13]([CH2:2][C:3]1[S:4][C:5]([N+:8]([O-:10])=[O:9])=[CH:6][CH:7]=1)([O:14][CH3:15])=[O:16]

참가 물질

3

반응물 2

HCID 8472Trimethyl phosphiteHCID 536851562-(Bromomethyl)-5-nitrothiophene

생성물 1

HCID 197005052-Dimethoxyphosphorylmethyl-5-nitrothiophene

실험 절차

2-Bromomethyl-5-nitrothiophene and trimethylphosphite ((CH3O)3 P) were treated in the same manner as in Reference Example 43 to yield 2-dimethoxyphosphorylmethyl-5-nitrothiophene as an oil.

출처 및 근거

ORD 기록
ord-3c413eb989ee424b802a5f153e1958b6
출처 데이터셋
uspto-grants-1998_02
특허 번호
US05716944

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