Formaldehyde → Resorcinol-formaldehyde resin

HRID 862140

반응식

HRID 862140 반응식
[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].C=O>>[CH2:1]=[O:2].[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2]

참가 물질

3

반응물 2

HCID 712FormaldehydeHCID 5054Resorcinol

생성물 1

HCID 159980Resorcinol-formaldehyde resin

실험 절차

In a four-necked flask equipped with a reflux condenser and a thermometer were placed 110 g (1.0 mole) of resorcin and 44.5 g (0.55 mole) of 37% formalin, and the resulting mixture was subjected to reaction at 70° C. for five hours. The reflux condenser was then replaced by a fractionator, and the pressure in the flask was reduced to 25 mmHg, after which the temperature was elevated to 150° C., at which temperature the contents of the flask were concentrated for three hours to obtain a resorcin formaldehyde resin [T].

후처리

  1. customIn a four-necked flask equipped with a reflux condenser
  2. customthe resulting mixture was subjected to reaction at 70° C. for five hours
  3. customwas elevated to 150° C., at which temperature
  4. concentrationwere concentrated for three hours

출처 및 근거

ORD 기록
ord-fabe99119f714e16a297ecd700467720
출처 데이터셋
uspto-grants-1998_02
특허 번호
US05717053

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