Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-Butylamine → 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-Butylamine | HCID 6385 | — |
| 반응물 | 3-Cyanoandrosta-3,5-diene-17beta-carboxylic acid | HCID 15380254 | — |
| 생성물 | 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide | HCID 67646951 | 81% |
반응 단계
Following a procedure similar to that described in Preparation 16a, but using 3-cyanoandrosta-3,5-diene-17β-carboxylic acid [prepared as described in Example 1(b)] and t-butylamine as starting materials, in relative proportions similar to those used in that Preparation, the title compound was obtained in a yield of 81%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05717088 |
| 출처 데이터셋 | uspto-grants-1998_02 |
| ORD ID | ord-0dbbd67c48fd4b9db0ae66e1af54153b |
| 출처 메모 | uspto-grants-1998_02 |