Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → 1,3-Bis(2-t-amylperoxy-2-propyl)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | p-Bis(2-hydroxyisopropyl)benzene | HCID 18062 | — |
| 반응물 | tert-Amyl hydroperoxide | HCID 76962 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1,3-Bis(2-t-amylperoxy-2-propyl)benzene | HCID 54131583 | — |
반응 단계
1,4-Bis(2-t-amylperoxy-2-propyl)benzene (para III) was prepared by reacting 28.1 grams (0.231 mole) of aqueous 85.7% t-amyl hydroperoxide diluted with 3.2 grams of water with 20.4 grams (0.105 mole) of 1,4-bis(2-hydroxy-2-propyl)benzene in the presence of 44.1 grams (0.316 mole) of 70% sulfuric acid according to the procedure of Example VII. The stripped product was a yellow liquid which remained liquid at 15° C. The product weighed 32.0 grams.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05719096 |
| 출처 데이터셋 | uspto-grants-1998_02 |
| ORD ID | ord-ccabd420d1484ab6a9d0f8a6e1052f08 |
| 출처 메모 | uspto-grants-1998_02 |