Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → N-(2-pyridylmethyl)benzhydrylsulphinylacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | 2-Pyridinemethanamine | HCID 19509 | — |
| 반응물 | Modafinil acid | HCID 3085267 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-(2-pyridylmethyl)benzhydrylsulphinylacetamide | HCID 15225687 | — |
반응 단계
To a suspension of 15.44 g (0.06 mol) of benzhydrylsulphinylacetic acid in 90 ml of methylene chloride are added 6.48 g (0.06 mol, i.e. 6.17 ml) of 2-aminomethylpyridine and 12.36 g (0.06 mol) of dicyclohexylcarbodiimide are added to the solution thus obtained. The mixture is heated at reflux for about 3 to 4 hours, then left to cool.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05719168 |
| 출처 데이터셋 | uspto-grants-1998_02 |
| ORD ID | ord-6769afe3f93e45529751b5d6b490635d |
| 출처 메모 | uspto-grants-1998_02 |