Hexane → 4-(2-Phenylbenzoylamino)-benzoylchloride

HRID 863037노트

반응식

HRID 863037 반응식
[C:1]1([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:2]([C:7]([NH:9][C:10]2[CH:18]=[CH:17][C:13]([C:14](O)=[O:15])=[CH:12][CH:11]=2)=[O:8])=[CH:3][CH:4]=[CH:5][CH:6]=1.CCCCCC.S(Cl)([Cl:33])=O>>[C:1]1([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:2]([C:7]([NH:9][C:10]2[CH:18]=[CH:17][C:13]([C:14]([Cl:33])=[O:15])=[CH:12][CH:11]=2)=[O:8])=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

4

반응물 3

HCID 8058HexaneHCID 24386Thionyl ChlorideHCID 105435024-[(2-phenylbenzoyl)amino]benzoic Acid

생성물 1

HCID 114505014-(2-Phenylbenzoylamino)-benzoylchloride

실험 절차

A mixture of 1.39 g of 4-[([1,1'-biphenyl]-2-carbonyl)amino]benzoic acid in 2.0 ml of thionyl chloride is heated on a steam bath for 1 hour. Cold hexane is added and the crystalline solid collected and dried to give 1.34 g of the desired product, m.p. 118°-120° C.

후처리

  1. temperatureis heated on a steam bath for 1 hour
  2. customthe crystalline solid collected
  3. customdried

출처 및 근거

ORD 기록
ord-301216aaebbd4eea9d44b3c93bc38501
출처 데이터셋
uspto-grants-1998_02
특허 번호
US05719278

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