Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfate → N-(7-methoxynaphthalen-1-yl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfate | HCID 6497 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-Acetamido-7-naphthol | HCID 80946 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | N-(7-methoxynaphthalen-1-yl)acetamide | HCID 11447230 | — |
반응 단계
A mixture of 8-Acetamido-2-naphthol (21 g, 0.104 mol), dimethyl sulfate (15.1 g, 0.12 mol) and potassium carbonate (41 g, 0.3 mol) in acetone (200 mL) was stirred at room temperature for 48 h. Solids were removed by filtration and washed with methanol, and the filtrate evaporated. The residue was washed in 1:1 hexane:toluene, collected by filtration and dried (24.7 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05721234 |
| 출처 데이터셋 | uspto-grants-1998_02 |
| ORD ID | ord-6af2e0d4890a4fea8e82f0200997e77e |
| 출처 메모 | uspto-grants-1998_02 |