Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Leucinamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Leucinamide hydrochloride | HCID 2733199 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylacetamide | HCID 31374 | — |
| 생성물 | Leucinamide | HCID 69640 | — |
반응 단계
1.25M solution of Leu-NH2 in DMAC was prepared by dissolving Leu-NH2.HCl (1.33 g, 7.98 mmol) in 5.0 mL of water, titrating to pH 8.0 with 1M NaOH, lyophilizing, and taking up the residue in 6.4 ml of DMAC. The NaCl precipitate was removed by filtering through a fine glass frit to give a clear solution of pH 9.25.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05563044 |
| 출처 데이터셋 | uspto-grants-1996_10 |
| ORD ID | ord-b5d127ef1e6044608b68a102b37d5fbf |
| 출처 메모 | uspto-grants-1996_10 |