Chloride → 2-Methyl-3,4,6-trifluorobenzoyl chloride

반응식

[CH3:1][C:2]1[C:10]([F:11])=[C:9]([F:12])[CH:8]=[C:7]([F:13])[C:3]=1[C:4](O)=[O:5].[Cl-:14]>>[CH3:1][C:2]1[C:10]([F:11])=[C:9]([F:12])[CH:8]=[C:7]([F:13])[C:3]=1[C:4]([Cl:14])=[O:5]

참가 물질

반응물 2

HCID 312Chloride

HCID 101303052-Methyl-3,4,6-trifluorobenzoic acid

생성물 1

HCID 150076072-Methyl-3,4,6-trifluorobenzoyl chloride

실험 절차

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

후처리

temperaturethe mixture is refluxed for hour
concentrationAfter concentrating

출처 및 근거

ORD 기록: ord-e4be45eaf8604950a34e32fb6ac79133
출처 데이터셋: uspto-grants-1996_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05563138

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