Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,5-Dichlorophenol → 2,5-Dichlorophenyl Dimethyloctylsilyl Ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,5-Dichlorophenol | HCID 66 | — |
| 반응물 | Imidazole | HCID 795 | — |
| 반응물 | Chlorodimethyloctylsilane | HCID 87482 | — |
| 용매 | Sodium Chloride | HCID 5234 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2,5-Dichlorophenyl Dimethyloctylsilyl Ether | HCID 53988840 | — |
반응 단계
To a solution of 3.75 g (0.023 mole) 2,5-dichlorophenol in 30 ml N,N-dimethylformamide are added 5.58 g (0.082 mole) imidazole and 16.6 ml (0.070 mole) chlorodimethyloctyl silane under argon. After stirring at room temperature for two hours, the mixture is diluted with an aqueous saturated sodium chloride solution and extracted with ether. The combined organic extracts are dried and condensed. The product is purified by column chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05565543 |
| 출처 데이터셋 | uspto-grants-1996_10 |
| ORD ID | ord-c6e4eef05fd94331a9e1f324b60fab4a |
| 출처 메모 | uspto-grants-1996_10 |