Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-dimethyl-5-nitropyridin-2-amine → HCID 178482865, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-dimethyl-5-nitropyridin-2-amine | HCID 75707 | — |
| 반응물 | Diphenyl N-Cyanocarbonimidate | HCID 688090 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | HCID 178482865 | HCID 178482865 | 74.4% |
반응 단계
A stirred mixture of the crude amine prepared from 5.00 g (0.0299 mol) of the product from Step 1, diphenylcyanocarbonimidate (7.20 g, 0.0302 mol) and ethylene glycol dimethyl ether (60 ml) was kept under nitrogen for 3 hours and diluted with Et20. The solid was collected by filtration, washed with Et2O and dried to give 6.26 g of the titled product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05567722 |
| 출처 데이터셋 | uspto-grants-1996_10 |
| ORD ID | ord-15d7e9c2f2fb45e3b9b7e58347d30634 |
| 출처 메모 | uspto-grants-1996_10 |