Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 4-(Benzyloxy)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Benzyl p-tolyl ether | HCID 70036 | — |
| 용매 | Sodium Dichromate | HCID 25408 | — |
| 생성물 | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
반응 단계
A mixture of 4-methylphenoxy phenyl methane (2g) was suspended in aqueous sodium dichromate solution (20ml. 50%) and concentrated sulphuric acid (10ml) added dropwise with stirring. The mixture was stirred at room temperature overnight then warmed on a water bath for 1hr. The mixture was cooled, diluted with water and the 4-carboxyphenoxy phenyl methane (m.p. 188°) isolated with ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04098816 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-ae4c4a93c7aa4cb593dbf89f125d6d34 |
| 출처 메모 | uspto-grants-1978_07 |