참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nicotinic Acid | HCID 938 | — |
| 반응물 | Benzoguanamine | HCID 7064 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-Amino-4-nicotinamido-6-phenyl-s-triazine | HCID 14601634 | — |
| 생성물 | 2,4-Bis(nicotinamido)-6-phenyl-s-triazine | HCID 20321035 | — |
반응 단계
1.9 g of benzoguanamine and 2.6 g of nicotinic acid are dissolved in 50 ml of pyridine, and the mixture is further mixed with 2.5 g of methanesulfonyl chloride and agitated at 60° C for 3 hours. Following processing as described in Example 4, there is obtained 0.11 g of 2-amino-4-nicotinamido-6-phenyl-s-triazine [mononicotinoylbenzoguanamine] and 1.05 g of 2,4-bis(nicotinamido)-6-phenyl-s-triazine (dinicotinoylbenzoguanamine).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04098892 |
|---|
| 출처 데이터셋 | uspto-grants-1978_07 |
|---|
| ORD ID | ord-ac26d0f05938438796fbe85d5d4447e0 |
|---|
| 출처 메모 | uspto-grants-1978_07 |
|---|
