Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine → 3-(Cyclohexyldisulfanyl)-2-methylfuran
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine | HCID 807 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Cyclohexanethiol | HCID 15290 | — |
| 반응물 | 2-Methyl-3-furanthiol | HCID 34286 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3-(Cyclohexyldisulfanyl)-2-methylfuran | HCID 20313890 | — |
반응 단계
0.57 Grams (0.0050 moles) of 2-methyl-3-furanthiol and 1.16 grams (0.01 moles) of cyclohexylmercaptan are dissolved in 12 ml of diethyl ether. 0.8 Grams (0.0075 moles) of sodium carbonate dissolved in 8 ml water is added to the reaction mass. Over a period of 10 minutes, a solution of 1.9 grams (0.0075 moles) of iodine dissolved in 6 ml diethyl ether is added to the reaction mass with stirring until the iodine color remains. The reaction mass is then stirred over a period of 45 minutes.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04098910 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-5bf50225e8f643f8bec01a20944659ad |
| 출처 메모 | uspto-grants-1978_07 |