Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 20382795, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Succinic anhydride | HCID 7922 | — |
| 반응물 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 반응물 | Oxalic acid, dihydrazide | HCID 13826 | — |
| 생성물 | HCID 20382795 | HCID 20382795 | 49% |
반응 단계
Two moles (200 g.) of succinic anhydride and one mole (118 g.) of oxalic dihydrazide in 750 ml. N-methyl-2-pyrrolidone and 500 ml. toluene were heated at reflux until water evolution was complete (about 4 hours). Upon cooling, a crystalline complex separated. The mixture was diluted with benzene and then filtered. After drying at 50° C, the complex was treated with water to give N,N'-bis(succinimido)oxamide, having a melting point of >310° C. The overall yield was about 49%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04100132 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-87418fde660d413491dd8ff98aee3fdb |
| 출처 메모 | uspto-grants-1978_07 |