Triethylenetetramine → HCID 20319855, 화합물

HRID 866713

반응식

HRID 866713 반응식
[ClH:1].Cl.Cl.C12CCC(CC1)CC2CC(NCCCNCCCN)CC1C[CH:19]2[CH2:21][CH2:22][CH:16]1[CH2:17][CH2:18]2.C12C[CH2:38][CH:35](CC1)[CH2:34][CH:33]2[CH2:40][C:41](=O)[CH2:42][CH:43]1[CH2:48][CH:47]2[CH2:49][CH2:50][CH:44]1[CH2:45][CH2:46]2.[CH2:52]([CH2:55][NH:56][CH2:57][CH2:58][CH2:59][NH2:60])[CH2:53][NH2:54].Cl.Cl.Cl.Cl.C12CCC(CC1)CC2CC(NCCNCCNCCN)CC1CC2CCC1CC2.NCCNCCNCCN.C12CCC(CC1)CC2CCCC(=O)CCCC1CC2CCC1CC2.Cl.Cl.Cl.C12CCC(CC1)CC2C(CC(NCCCNCCCN)CC(C1CC2CCC1CC2)C)C.C12CCC(CC1)CC2C(CC(=O)CC(C1CC2CCC1CC2)C)C>>[ClH:1].[ClH:1].[ClH:1].[CH:44]12[CH2:45][CH2:46][CH:47]([CH2:49][CH2:50]1)[CH2:48][CH:43]2[CH2:42][CH2:41][CH:40]([NH:54][CH2:53][CH2:52][CH2:55][NH:56][CH2:57][CH2:58][CH2:59][NH2:60])[CH2:33][CH2:34][CH:35]1[CH2:38][CH:16]2[CH2:17][CH2:18][CH:19]1[CH2:21][CH2:22]2

참가 물질

9

반응물 8

HCID 5565TriethylenetetramineHCID 5942Bis(3-aminopropyl)amine3회HCID 20319799HCID 20319799, 화합물HCID 20319811HCID 20319811, 화합물HCID 20319815HCID 20319815, 화합물HCID 20319831HCID 20319831, 화합물HCID 20319859HCID 20319859, 화합물HCID 20319869HCID 20319869, 화합물2회

생성물 1

HCID 20319855HCID 20319855, 화합물

실험 절차

Also prepared by this method in an analogous manner regarding molar quantities and reaction conditions are 1-[1,3-di-(bicyclo[2.2.2]oct-2-yl)-2-propyl]-1,5,9-triazanonane trihydrochloride from 1,3-di-(bicyclo[2.2.2]oct-2-yl)-2-propanone and 3,3'-iminobispropylamine; 1-[1,3-di-(bicyclo[2.2.2]oct-2-yl)-2-propyl]-1,4,7,10-tetraazadecane tetrahydrochloride from 1,3-di-(bicyclo[2.2.2]oct-2-yl)-2-propanone and triethylenetetramine; 1-[1,7-di-(bicyclo[2.2.2-oct-2-yl)-4-heptyl]-1,5,9-triazanonane trihydrochloride from 1,7-di-(bicyclo[2.2.2]oct-2-yl)-4-heptanone and 3,3'-iminobispropylamine and 1-[2,6-di-(bicyclo[2.2.2]oct-2-yl)-4-heptyl]-1,5,9-triazanonane trihydrochloride from 2,6-di-(bicyclo[2.2.2]oct-2-yl)-4-heptanone and 3,3'-iminobispropylamine.

후처리

  1. customAlso prepared by this method in an analogous manner
  2. customquantities and reaction conditions

출처 및 근거

ORD 기록
ord-a1f136ac7e3c4ff588c9dff8e6ce5c0a
출처 데이터셋
uspto-grants-1978_07
특허 번호
US04100193

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