Methanol → 1,1-Dimethoxy-3-(methylthio)propane

HRID 866716노트

반응식

HRID 866716 반응식
[CH3:1][S:2][CH2:3][CH2:4][CH:5]=[O:6].[C:7]1(C)C=CC(S(O)(=O)=O)=CC=1.[CH3:18][OH:19]>>[CH3:18][O:19][CH:5]([O:6][CH3:7])[CH2:4][CH2:3][S:2][CH3:1]

참가 물질

4

반응물 3

HCID 887MethanolHCID 6101p-Toluenesulfonic acidHCID 18635Methional

생성물 1

HCID 832401,1-Dimethoxy-3-(methylthio)propane

실험 절차

20.8 g (0.2 mole) of freshly distilled methional and 100 cc of methyl alcohol are heated under reflux in the presence of 0.5 g of p-toluene sulphonic acid.

출처 및 근거

ORD 기록
ord-74292e945ace4c5da8ac89b874ff66ab
출처 데이터셋
uspto-grants-1978_07
특허 번호
US04101307

반응 노트

불러오는 중…