Water → 4-Aminocinnamonitrile

HRID 866745노트

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HRID 866745 반응식
[N+:1]([C:4]1[CH:13]=[CH:12][C:7]([CH:8]=[CH:9][C:10]#[N:11])=[CH:6][CH:5]=1)([O-])=O.O>C(O)C>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([CH:8]=[CH:9][C:10]#[N:11])=[CH:12][CH:13]=1

참가 물질

4

반응물 2

HCID 962WaterHCID 34056p-Nitrocinnamonitrile

생성물 1

HCID 545249384-Aminocinnamonitrile수율 76%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The 4-nitro-cinnamonitrile thus obtained is then reduced by the Bechamp reaction in 2000 parts of water and 800 parts of ethyl alcohol. 4-amino-cinnamonitrile which melts at 109°-110° C. is thus obtained. Yield: 76%.

출처 및 근거

ORD 기록
ord-4752308f933247ffb4e9d8967254ff25
출처 데이터셋
uspto-grants-1978_07
특허 번호
US04101543

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