Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → N-benzhydryl-N'-methylthiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Benzhydryl isothiocyanate | HCID 520742 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | N-benzhydryl-N'-methylthiourea | HCID 3442043 | — |
반응 단계
A solution of 13.50 g (0.06 Mole) of benzhydrylisothiocyanate in ether is saturated with anhydrous methylamine in an ice bath. The crystals are filtered to yield the product, N-benzhydryl-N'-methylthiourea; mp 152°-154° C, which is sufficiently pure for the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04101659 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-7d89f92d550b4f6b82ec1dea8e722a52 |
| 출처 메모 | uspto-grants-1978_07 |