Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 1-Amino-6-nitroanthracene-9,10-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 1,6-Dinitroanthraquinone | HCID 74146 | — |
| 용매 | Pentane | HCID 8003 | — |
| 생성물 | 1-Amino-6-nitroanthracene-9,10-dione | HCID 20317509 | 91.5% |
반응 단계
310 g of 1,6-dinitroanthraquinone (96%) were reacted 0.5 hours with 340 g of ammonia (molar ratio 20:1; pressure 80 atms) in 1 liter of n-pentane in an autoclave at 150° C.; the reaction mixture obtained was freed from the solvent by distillation. Residue: 269 g of a 91.5% 1-amino-6-nitroanthraquinone (89% of the theoretical yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04102906 |
| 출처 데이터셋 | uspto-grants-1978_07 |
| ORD ID | ord-5606c31aadb54e47b3ef2ddf514ad31c |
| 출처 메모 | uspto-grants-1978_07 |