Potassium Hydroxide → HCID 13882128, 화합물

HRID 867376노트

반응식

HRID 867376 반응식
[C:1]([C:3]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:6]=[CH:5][C:4]=1[C:14]([O:16]CC)=[O:15])#[N:2].[OH-:19].[K+]>C(O)C>[C:14]([C:4]1[CH:5]=[N:6][N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:3]=1[C:1]([NH2:2])=[O:19])([OH:16])=[O:15]

참가 물질

4

반응물 2

HCID 14797Potassium HydroxideHCID 13772968Ethyl 5-cyano-1-phenyl-1H-pyrazole-4-carboxylate

생성물 1

HCID 13882128HCID 13882128, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A 4 g. portion of ethyl 5-cyano-1-phenyl-4-pyrazolecarboxylate was reacted with 2 g. of potassium hydroxide in 60 ml. of denatured ethanol substantially as described in Example 2, to obtain 2.7 g. of the desired product, m.p. 234°-235°, having the following elemental analysis.

후처리

  1. customto obtain 2.7 g

출처 및 근거

ORD 기록
ord-9a46a9ba0c5f4348b6a608989697f618
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04775409

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