Pyridine, 3-(1H-1,2,3-triazol-1-yl)- (9CI) → HCID 21290348, 화합물

HRID 867628노트

반응식

HRID 867628 반응식
[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5](N2C=CN=N2)[CH:6]=[N:7][CH:8]=1.[N:16]1(C2C=NC=CC=2)[CH:20]=[CH:19][N:18]=[N:17]1.ClC1C=C(N2C=CN=N2)C=C(Cl)N=1.ClC1C=C(N2C=CN=N2)C=C(C(F)(F)F)N=1.ClC1C(Cl)=C(N2C=CN=N2)C(Cl)=C(Cl)N=1>>[F:15][C:2]([F:1])([F:14])[C:3]1[CH:4]=[CH:5][C:6]([N:16]2[CH:20]=[CH:19][N:18]=[N:17]2)=[N:7][CH:8]=1

참가 물질

6

반응물 5

HCID 18794854Pyridine, 3-(1H-1,2,3-triazol-1-yl)- (9CI)HCID 21290340HCID 21290340, 화합물HCID 21290341HCID 21290341, 화합물HCID 21290346Pyridine, 3-(1H-1,2,3-triazol-1-yl)-5-(trifluoromethyl)-HCID 21290360HCID 21290360, 화합물

생성물 1

HCID 21290348HCID 21290348, 화합물

실험 절차

The following were prepared analogously and identified by NMR spectroscopy and elemental (CHN) analysis: 5-(trifluoromethyl)-3-(1H-1,2,3-triazol-1-yl)pyridine, m.p. 129.5°-131° C.; 3-(1H-1,2,3-triazol-1-yl)pyridine, m.p. 80.5°-83° C.; 2,6-dichloro-4-(1H-1,2,3-triazol-1-yl)pyridine, m.p. 80°-83° C.; 2-chloro-6-(trifluoromethyl)-4-(1H-1,2,3-triazol-1-yl)pyridine, and 2,3,5,6-tetrachloro-4-(1H-1,2,3-triazol-1-yl)pyridine, m.p. 161°-162.5° C.

후처리

  1. customThe following were prepared analogously

출처 및 근거

ORD 기록
ord-1091fbbb5be64f07a978de0286b6e96f
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04775762

반응 노트

불러오는 중…