Water → HCID 14273353, 화합물
반응식
[C:1](=[O:18])([O:10]CC1C=CC=CC=1)[O:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH3:19][N:20]([CH3:22])[CH3:21].O>CO>[C:1](=[O:2])([O-:18])[OH:10].[CH3:19][N+:20]([CH3:22])([CH3:21])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1참가 물질
5
실험 절차
101.6 g of dibenzyl carbonate, 23.6 g of trimethylamine, 60.5 g of water and 20.0 g of methanol were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 150° C., the reaction was continued for 5 hours at 150° C. Trimethylbenzylammonium hydrogencarbonate was obtained in a yield of 81.0 mol % (based on trimethylamine).
후처리
- customas used in Preparation Example 1
- temperatureheated
- customreached 150° C.
출처 및 근거
- ORD 기록
- ord-9286e326111948b38f720d509211f04d
- 출처 데이터셋
- uspto-grants-1988_10
- 특허 번호
- US04776929
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