AGN-PC-0NC49B → HCID 14273353, 화합물
반응식
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:16])([CH3:15])[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:16])([CH3:15])[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1참가 물질
3
시약·촉매·용매 1
실험 절차
112.5 g of trimethylbenzylammonium monomethylcarbonate and 55.0 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylbenzylammonium hydrogencarbonate was obtained in a yield of 95.7 mol %.
후처리
- customas used in Preparation Example 1
- temperatureheated
- customreached 120° C.
출처 및 근거
- ORD 기록
- ord-7f7da973e61b4a93aa39d8f9bc886d11
- 출처 데이터셋
- uspto-grants-1988_10
- 특허 번호
- US04776929
반응 노트
불러오는 중…