HCID 19871551, 화합물 → HCID 85570074, 화합물
반응식
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]참가 물질
3
시약·촉매·용매 1
실험 절차
114.1 g of trimethylethylammonium monomethylcarbonate and 75.6 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylethylammonium hydrogencarbonate was obtained in a yield of 96.3 mol %.
후처리
- customas used in Preparation Example 1
- temperatureheated
- customreached 120° C.
출처 및 근거
- ORD 기록
- ord-13ae56ff8ff94768903a653a32d808d9
- 출처 데이터셋
- uspto-grants-1988_10
- 특허 번호
- US04776929
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