Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Pyridineethanamine → 1,8,8-Trimethyl-3-[2-(2-pyridinyl)ethyl]-3-azabicyclo[3.2.1]octane-2,4-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Pyridineethanamine | HCID 75919 | — |
| 반응물 | 1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione | HCID 94834 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 1,8,8-Trimethyl-3-[2-(2-pyridinyl)ethyl]-3-azabicyclo[3.2.1]octane-2,4-dione | HCID 14235066 | — |
반응 단계
A mixture of (-) camphoric anhydride 5 g (0.029 mol), 2-(2-aminoethyl)pyridine 3.6 (0.03 mol) and 50 ml of pyridine was refluxed overnight. The solvent is removed under reduced pressure and the remaining oil boiled in 20 ml of ethanol and allowed to cool.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04777254 |
| 출처 데이터셋 | uspto-grants-1988_10 |
| ORD ID | ord-14d27eb0342e4f14801d1f2da1572273 |
| 출처 메모 | uspto-grants-1988_10 |