Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl phenyl ether → HCID 14328878, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl phenyl ether | HCID 74458 | — |
| 반응물 | 2-(1H-Imidazol-1-yl)-N-methyl-1-(2-naphthalenyl)ethanimine N-oxide | HCID 86742472 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 14328878 | HCID 14328878 | — |
반응 단계
A mixture of compound 2 (9.0 g, 0.034 mol) and phenyl allyl ether (6.98 ml, 0.051 mol) in 200 ml of toluene is refluxed for 48 hours, cooled and evaporated under vacuum. The semisolid that remained (7.30 g, 54%) is crystallized from ether and recrystallized from ethyl acetate to give tan crystals. Yield: 2.4 g (18%); m.p. 176°-178° C. (Found: C, 74.96; H, 6.41; N, 10.40. C25H25N3O2 requires: C, 75.16; H, 6.31; N, 10.52).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04777263 |
| 출처 데이터셋 | uspto-grants-1988_10 |
| ORD ID | ord-40739d68791d434b838e2b7febef88e8 |
| 출처 메모 | uspto-grants-1988_10 |