Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 54467230, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethyl 3-(3-hydroxy-5-hydroxymethyl-2-methyl-4-pyridyl)acrylate hydrochloride | HCID 67938271 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | HCID 54467230 | HCID 54467230 | 95.9% |
반응 단계
A mixture of 3.0 g of ethyl 3-(3-hydroxy-5-hydroxymethyl-2-methyl-4-pyridyl)acrylate hydrochloride in 15 ml of 1N aqueous sodium hydroxide solution is stirred at room temperature for 1 hour. The reaction mixture is adjusted to pH 4 with 10% hydrochloric acid, and the resulting precipitate is collected to give 2.2 g of 3-(3-hydroxy-5-hydroxymethyl-2-methyl-4-pyridyl)acrylic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04778796 |
| 출처 데이터셋 | uspto-grants-1988_10 |
| ORD ID | ord-9fdfaace917c40dda78e7076ec6cc837 |
| 출처 메모 | uspto-grants-1988_10 |