참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethyl orthoacetate | HCID 66221 | — |
| 반응물 | 2-Chloro-3-hydrazinoquinoxaline | HCID 3658820 | — |
| 생성물 | 4-Chloro-1-methyl[1,2,4]triazolo[4,3-a]quinoxaline | HCID 2768643 | — |
반응 단계
A reaction mixture of 5 g of 2-chloro-3-hydrazinoquinoxaline in 50 ml of triethyl orthoacetate was heated at 100° C. for three hours. Upon cooling, the precipitated solid was filtered, washed with cyclohexane, and dried affording 4.27 g of 4-chloro-1-methyl[1,2,4]triazolo[4,3-a]quinoxaline having a mp of 215°-218° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04780464 |
|---|
| 출처 데이터셋 | uspto-grants-1988_10 |
|---|
| ORD ID | ord-2e1c081b3c124ed88f2757f390ecb8b8 |
|---|
| 출처 메모 | uspto-grants-1988_10 |
|---|
