참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Chloro-3-hydrazinoquinoxaline | HCID 3658820 | — |
| 용매 | 1,1,1-Triethoxybutane | HCID 371779 | — |
| 생성물 | 4-Chloro-1-propyl[1,2,4]triazolo[4,3-a]quinoxaline | HCID 13385707 | — |
반응 단계
A reaction mixture of 5 g of 2-chloro-3-hydrazinoquinoxaline in 15 ml of triethyl orthobutyrate was heated at 100° C. for three hours. Upon cooling, the precipitated solid was filtered, washed with cyclohexane, and dried giving 4.0 g of 4-chloro-1-propyl[1,2,4]triazolo[4,3-aquinoxaline having a mp of 172°-175° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04780464 |
|---|
| 출처 데이터셋 | uspto-grants-1988_10 |
|---|
| ORD ID | ord-72bb7f62116c4883978918d06fff398e |
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| 출처 메모 | uspto-grants-1988_10 |
|---|
