Cyclopentylamine → N-Cyclobutyl-1-ethyl[1,2,4]triazolo[4,3-a]quinoxalin-4-amine

HRID 868520

반응식

Cl[C:2]1[C:3]2[N:4]([C:12]([CH2:15][CH3:16])=[N:13][N:14]=2)[C:5]2[C:10]([N:11]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2.[CH:17]1([NH2:21])[CH2:20][CH2:19][CH2:18]1.ClC1C2N(C(C)=NN=2)C2C(N=1)=CC=CC=2.C1(N)CCCC1>>[CH:17]1([NH:21][C:2]2[C:3]3[N:4]([C:12]([CH2:15][CH3:16])=[N:13][N:14]=3)[C:5]3[C:10]([N:11]=2)=[CH:9][CH:8]=[CH:7][CH:6]=3)[CH2:20][CH2:19][CH2:18]1

참가 물질

반응물 4

HCID 2906Cyclopentylamine

HCID 75645Cyclobutylamine

HCID 27686434-Chloro-1-methyl[1,2,4]triazolo[4,3-a]quinoxaline

HCID 133857064-Chloro-1-ethyl[1,2,4]triazolo[4,3-a]quinoxaline

생성물 1

HCID 14280614N-Cyclobutyl-1-ethyl[1,2,4]triazolo[4,3-a]quinoxalin-4-amine

실험 절차

The title compound was prepared essentially as described in Example 2 substituting 4-chloro-1-ethyl [1,2,4]triazolo[4,3-a]quinoxaline and cyclobutyl amine for 4-chloro-1-methyl[1,2,4]triazolo[4,3-a]quinoxaline and cyclopentanamine respectively; mp 215°-217° C.

출처 및 근거

ORD 기록: ord-39108676c506490cb37e88e5400d6891
출처 데이터셋: uspto-grants-1988_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04780464

연결된 노트

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