2-Chloroethyldiisopropylammonium chloride → HCID 13934419, 화합물

HRID 868568노트

반응식

HRID 868568 반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH3:13])[CH:5]=[C:6]2[C:10]=1[NH:9][C:8](=[O:11])[C:7]2=[O:12].Cl.[CH:15]([N:18]([CH:22]([CH3:24])[CH3:23])[CH2:19][CH2:20]Cl)([CH3:17])[CH3:16]>>[Br:1][C:2]1[CH:3]=[C:4]([CH3:13])[CH:5]=[C:6]2[C:10]=1[N:9]([CH2:20][CH2:19][N:18]([CH:22]([CH3:24])[CH3:23])[CH:15]([CH3:17])[CH3:16])[C:8](=[O:11])[C:7]2=[O:12]

참가 물질

3

반응물 2

HCID 779422-Chloroethyldiisopropylammonium chlorideHCID 6116217-Bromo-5-methylindoline-2,3-dione

생성물 1

HCID 13934419HCID 13934419, 화합물수율 13.1%

실험 절차

By using the 7-bromo-5-methylisatin and 2-diisopropylaminoethyl chloride hydrochloride, a method analogous to that described in Reference Example 1 was carried out to obtain 7-bromo-1-(2-diisopropylaminoethyl)-5-methylisatin having a melting point of 94°-97° C. (yield: 13.1%).

출처 및 근거

ORD 기록
ord-c46dc9e9b9d5495b9cdb70046daff00a
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04780477

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