Semicarbazide hydrochloride → HCID 178457307, 화합물

HRID 868587노트

반응식

HRID 868587 반응식
[CH:1]([N:4]([CH:19]([CH3:21])[CH3:20])[CH2:5][CH2:6][CH2:7][N:8]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:11](=O)[C:9]1=[O:10])([CH3:3])[CH3:2].Cl.[NH2:23][NH:24][C:25]([NH2:27])=[O:26]>>[CH:1]([N:4]([CH:19]([CH3:21])[CH3:20])[CH2:5][CH2:6][CH2:7][N:8]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)/[C:11](=[N:23]\[NH:24][C:25]([NH2:27])=[O:26])/[C:9]1=[O:10])([CH3:3])[CH3:2]

참가 물질

3

반응물 2

HCID 11236Semicarbazide hydrochlorideHCID 139344201-(3-Diisopropylaminopropyl)isatin

생성물 1

HCID 178457307HCID 178457307, 화합물수율 66.6%

실험 절차

By using 1-(3-diisopropylaminopropyl)isatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-1-(3-diisopropylaminopropyl)isatin 3-semicarbazone having a melting point of 173°-175° C. (yield: 66.6%, recrystallizing solvent: methanol-benzene).

출처 및 근거

ORD 기록
ord-6afa26a8e286416c9d4a471013b50dce
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04780477

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