Semicarbazide hydrochloride → HCID 178422541, 화합물

HRID 868590노트

반응식

HRID 868590 반응식
[CH:1]([N:4]([CH:19]([CH3:21])[CH3:20])[CH2:5][CH2:6][N:7]1[C:17]2[C:12](=[CH:13][C:14]([CH3:18])=[CH:15][CH:16]=2)[C:10](=O)[C:8]1=[O:9])([CH3:3])[CH3:2].Cl.[NH2:23][NH:24][C:25]([NH2:27])=[O:26]>>[CH:1]([N:4]([CH:19]([CH3:21])[CH3:20])[CH2:5][CH2:6][N:7]1[C:17]2[C:12](=[CH:13][C:14]([CH3:18])=[CH:15][CH:16]=2)/[C:10](=[N:23]\[NH:24][C:25]([NH2:27])=[O:26])/[C:8]1=[O:9])([CH3:3])[CH3:2]

참가 물질

3

반응물 2

HCID 11236Semicarbazide hydrochlorideHCID 13934409HCID 13934409, 화합물

생성물 1

HCID 178422541HCID 178422541, 화합물수율 53.9%

실험 절차

By using 1-(2-diisopropylaminoethyl)-5-methylisatin and semicarbazide hydrochloride, a method analogous to that described in Example 4 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)-5-methylisatin 3-semicarbazone having a melting point of 159°-161° C. (yield: 53.9%, recrystallizing solvent: chloroform-hexane).

출처 및 근거

ORD 기록
ord-4a6c65540ad14d73aff735467df2bc5e
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04780477

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