Semicarbazide hydrochloride → HCID 178487249, 화합물

HRID 868602노트

반응식

HRID 868602 반응식
[CH:1]([N:4]([CH:20]([CH3:22])[CH3:21])[CH2:5][CH2:6][N:7]1[C:17]2[C:12](=[CH:13][C:14]([O:18][CH3:19])=[CH:15][CH:16]=2)[C:10](=O)[C:8]1=[O:9])([CH3:3])[CH3:2].Cl.[NH2:24][NH:25][C:26]([NH2:28])=[O:27]>>[CH:1]([N:4]([CH:20]([CH3:22])[CH3:21])[CH2:5][CH2:6][N:7]1[C:17]2[C:12](=[CH:13][C:14]([O:18][CH3:19])=[CH:15][CH:16]=2)/[C:10](=[N:24]\[NH:25][C:26]([NH2:28])=[O:27])/[C:8]1=[O:9])([CH3:3])[CH3:2]

참가 물질

3

반응물 2

HCID 11236Semicarbazide hydrochlorideHCID 13934417HCID 13934417, 화합물

생성물 1

HCID 178487249HCID 178487249, 화합물수율 84%

실험 절차

By using 1-(2-diisopropylaminoethyl)-5-methoxyisatin and semicarbazide hydrochloride, a method analogous to that described in Example 6 was carried out to obtain (E)-1-(2-diisopropylaminoethyl)-5-methoxyisatin 3-semicarbazone having a melting point of 157°-159° C. (yield: 84.0%, recrystallizing solvent: ethanol).

출처 및 근거

ORD 기록
ord-043687bdb71c468ba549cad6ae30c09e
출처 데이터셋
uspto-grants-1988_10
특허 번호
US04780477

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