Hydrazine → 2,4-Dimethylbenzohydrazide
반응식
[CH3:1][C:2]1[CH:11]=[C:10]([CH3:12])[CH:9]=[CH:8][C:3]=1[C:4](OC)=[O:5].[NH2:13][NH2:14]>CO>[CH3:1][C:2]1[CH:11]=[C:10]([CH3:12])[CH:9]=[CH:8][C:3]=1[C:4]([NH:13][NH2:14])=[O:5]참가 물질
4
실험 절차
To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).
후처리
- temperaturethe mixture was heated
- temperatureunder reflux for 40 hours
- customThen the mixture was evaporated
- customdried under vacuum
출처 및 근거
- ORD 기록
- ord-f378556826b04b0b900242b1ebc2cb1b
- 출처 데이터셋
- uspto-grants-2015_03
- 특허 번호
- US08968708B2
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